Never put any object into the magnet except the NMR tube and spinner. No magnetic stirrer. Please prepare your samples outside the NMR facilities if possible. If you must use the NMR facility, please ...
The following guidelines will help with preparing 1.7mm tubes. Left to right: 600μl in a 5mm tube. 200μl in a 3mm tube, 3mm shigemi tube with 70μl and 30μl in a 1.7mm tube. 1 pence piece to scale ...
All samples submitted for service must be accompanied by a completed submission form. The majority of users of the NMR 3 facility receive training and use the spectrometers independently. However, ...
is therefore recommended to optimize NMR samples. These buffers usually contain salts (i.e. NaCl or KCl) which often increase protein solubility but may reduce signal to noise in cold NMR probes and ...
The Spinsolve uses standard 5 mm OD NMR test tubes, exactly the same as high field instruments, so sample handling is familiar and convenient. The instrument can be deployed in the lab where you ...
Have your data emailed to you when the acquisition is completed! Use this instrument for 1H, 19F, 19F{1H}, 13C, 11B, 31P, 29Si, 195Pt, or practically any "X" nucleus with automatic probe-tuning. This ...
Alexander Shekhtman, of SUNY-Albany, describes a novel technique called STINT-NMR (for structural interactions using in-cell NMR), which maps a protein?s structural changes in response to ...
This technique allows you to obtain concentration information about your NMR sample without the requirement of spiking with an internal calibrant. Selective Excitations Not sure which possible ...
The Nanalysis 60PRO benchtop NMR can be used with standard 5mm NMR tubes and standard NMR sample volumes. In addition, the permanent magnet eliminates the need for cryogens and weekly servicing. Five ...
For example, if you want to run the LCMS you must provide columns, sample vials, and mobile phase or if you want to run the NMR you must provide the NMR tubes and deuterated solvents. Most consumables ...
and from concentrated samples in just 10 seconds. The Spinsolve uses standard 5 mm OD NMR test tubes, exactly the same as high field instruments, so sample handling is familiar and convenient. The ...